Syntheses and Properties of Heterodinuclear μ-Ethynediyl Complexes Containing Palladium and Platinum

Abstract
Heterodinuclear μ-ethynediyl complexes Cl(R3P)2MC≡CM′(PR3)2Cl (3) (M = Pt, M′ = Pd; R = Me, Et, n-Bu) were prepared by the reactions of chloroethynylbis(trialkylphosphine)platinum (1) with dichlorobis(trialkylphosphine)palladium (2) in the presence of CuCl catalyst. These complexes were fully characterized by mass, 13C{1H}, and 31P{1H} NMR spectroscopies.

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