An Effective Method for the Preparation of ω-Bromoalkanols from α,ω-Diols
- 1 January 1985
- journal article
- research article
- Published by Georg Thieme Verlag KG in Synthesis
- Vol. 1985 (12) , 1161-1162
- https://doi.org/10.1055/s-1985-31464
Abstract
Pure ω-bromoalkanols 2 (n = 2-12), not contaminated by any dibromoalkanes or unreacted diols 1, were prepared in good yields by refluxing a mixture of diols 1, aqueous (48%) hydrogen bromide, and benzene using a Dean-Stark water separator.Keywords
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