Abstract
Benzene cis-trioxide has been pyrolysed in the gas phase in the temperature range 475–537 K. Only one product, all -cis-1, 4, 7-trioxacyclononatriene, was observed. First-order rate constants taken from the upper part of this range (515–537 K) fit the Arrhenius equation (i). The reaction is probably unimolecular and a detailed mechanism is discussed. log10(k/s–1)= 14.9 ± 0.6 –(176 900 ± 6 200 J mol–1)/RTln10 (i)

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