Abstract
An improved method for the determination of trace quantities of free cyanide has been developed using ion chromatography with electrochemical detection. Detection limits of 1 μg/L have been achieved with linearity of response over the range 1 to 1000 μg/L. The precision of replicate injections is 0.6 percent, expressed as the relative standard deviation. The method has been applied to the analysis of dust samples.

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