The synthesis and purification of pentylenetetrazole‐10‐14C
- 1 January 1970
- journal article
- Published by Wiley in Journal of Labelled Compounds and Radiopharmaceuticals
- Vol. 6 (1) , 40-44
- https://doi.org/10.1002/jlcr.2590060106
Abstract
Pentylenetrazole‐10‐14C was synthesized by reacting hydrazoic acid with cyclohexanone‐1‐14C. Purification was carried out using sublimation and thick layer chromatography. Proof of radiochemical purity was determined using thin layer chromatography and autoradiography. The specific activity was found using liquid scintillation counting.Keywords
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- Über den Imin‐RestBerichte der deutschen chemischen Gesellschaft (A and B Series), 1924