121Sb Mössbauer Spectroscopy: Stereochemical Activity of the 5s Electrons in some Sb(III) Halide Complexes

Abstract
The 121Sb Mössbauer spectra of a number of SbX4 and Sb2X93− salts have been recorded. Only SbF4, SbCl4, and Sb2F93− show significantly large quadrupole splittings with the 5s electrons being stereochemically active.

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