Abstract
Polarisation of 19F-nuclei during the insertion of triplet diphenylmethylene into the benzylic C–H bond of individual, optically active, diastereoisomeric 1-methyl-heptyl α-fluorophenylacetates appears equally in both diastereoisomeric products, indicating that the radical pairs giving rise to CIDNP show no stereochemical preference in their combination.

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