A Convenient, Short Synthesis of (E)-1,3-Butadienyl(tributyl)stannane
- 1 January 1993
- journal article
- research article
- Published by Georg Thieme Verlag KG in Synthesis
- Vol. 1993 (10) , 943-944
- https://doi.org/10.1055/s-1993-25971
Abstract
A ready two-step procedure for medium scale preparation of (E)-1, 3-butadienyl(tributyl)stannane involves stannylation (Bu3SnI-lithium hexamethyldisilazide) of 2,5-dihydrothiophene S,S-dioxide (3-sulfolene) followed by thermal extrusion of sulfur dioxide.Keywords
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