Abstract
Depending on the pH and the respective concentrations of solutions containing NH4+/NH3/H2O2/NH4VO3 three yellow ammonium salts can be isolated: (NH4)4[O(VO(O2)2)2], NH4[VO(O2)2NH3]; and the novel (NH4)3[HV2O11] · 2 H2O. A cesium and potassium salt of the latter anion have been prepared. The infrared spectra of these salts are interpreted assuming a μ-hydroxo-bis[oxo-diperoxovanadate(V)] structure in the solid state.

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