A SPECTROPHOTOMETRIC DETERMINATION OF TRACES OF PHENOLIC STEROIDS IN 3-KETOSTEROIDS

Abstract
As little as 0ṁ02 per cent of phenolic steroid may be determined in the presence of an excess of 3-ketosteroid. The interfering ketonic absorption is eliminated by selective reduction of ketone by potassium borohydride. The slight absorption of the reduction products may be corrected graphically.

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