Crystal structure of Hexakis(hydroxylamine-N)nickel(II) sulphate
- 1 January 1974
- journal article
- Published by CSIRO Publishing in Australian Journal of Chemistry
- Vol. 27 (3) , 503-507
- https://doi.org/10.1071/ch9740503
Abstract
The crystal structure of the title compound, [Ni(NH20H)6] SO4, has been determined at 298 K by photographic methods; the structure was solved by the heavy atom method and refined by block diagonal least-squares procedures to a residual of 0.095 (1166 independent reflections). Crystal data: triclinic, PI, a 14.026(3), b 6.741(2), c 6.358(1) �, α-98.35(2), β 79.57(1), γ 95.06(2)�, Z 2. In the two crystallographically independent centrosymmetric cations, the nickel atoms are octahedrally coordinated by the ligand nitrogen atoms, (Ni-N), 2.12 �,Keywords
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