Abstract
Milk heated in sealed cans for 1- and 2-hr. periods at 116[degree]C was analyzed for formic acid by the A. O. A. C. distillation procedure. In addition, formic acid measurements were made on milk to which known amts. of formic acid were added. Results revealed that 60-71% of the added formic acid was recovered by the method used, with an av. recovery of 66.5%. In milk heated for 1 hr., the formic acid represented approx. 49% of the total titrable acidity increase when the retention correction was used. Milk heated for 2 hrs. contained an amt. of formic acid equivalent to approx. 57% of the titrable acidity increase.