Cyclometallation reactions. XV. ortho-Metallation of a sulphur-donor ligand

Abstract
The reaction between benzyl methyl sulphide and Mn(CH2Ph)(CO)5 affords the ortho-metallated-complex Mn(C6H4CH2SMe)(CO)4. Some other, non- metallated complexes of the sulphur-donor ligand with ruthenium and palladium are described; with rhenium, a complex disproportionation reaction occurs, apparently giving mixed [Re(CO)3(SR)]4 (R = Me, Ph or CH2Ph) complexes.

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