Synthesis and Crystal Structure Determination of a λ3 Pλ5 P-Phosphorane of a Novel Type
Open Access
- 1 June 1983
- journal article
- Published by Walter de Gruyter GmbH in Zeitschrift für Naturforschung B
- Vol. 38 (6) , 702-704
- https://doi.org/10.1515/znb-1983-0609
Abstract
The synthesis of a λ3 P-substituted phosphorane involving direct substitution of a Ph2P group at λ5P by the reaction of a chlorophosphorane with Ph2PSiMe3 is described; the identity of this novel compound is established by NMR and mass spectroscopy, and by a single crystal X-ray diffraction study.Keywords
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