THE CRYSTAL STRUCTURE AND ABSOLUTE CONFIGURATION OF (+)-O-METHYL-O-(α-NAPHTHYL)-S-METHYL PHOSPHOROTHIOLATE
- 1 March 1983
- journal article
- research article
- Published by Taylor & Francis in Phosphorus and Sulfur and the Related Elements
- Vol. 15 (1) , 105-108
- https://doi.org/10.1080/03086648308073284
Abstract
The structure of the title compound was solved by routine direct method and refined to R = 0.047 for 1422 independent reflections. The absolute configuration at phosphorus was found to be R. C12H13O3PS, orthorombic, P212121, a = 6.967(1), b = 10.600(2), c = 17.656(2) A, z = 4, V = 1303.90 Å3, Dc = 1.374 g·cm−3, μ = 3.6 cm−1 (MoKα).Keywords
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