Synthesis ofO-Alkyl Carbonochloridothioates
- 1 January 1986
- journal article
- research article
- Published by Georg Thieme Verlag KG in Synthesis
- Vol. 1986 (09) , 760-761
- https://doi.org/10.1055/s-1986-31767
Abstract
The preparation of O-alkyl carbonochloridothioates (2) was improved by performing the reaction of thiophosgene with potassium alkoxides in the corresponding alcohol or in tetrahydrofuran at - 65°C for 1 hour. In all cases, the reaction yielded products 2, O,O-dialkyl carbonothioates (4), and dialkyl carbonates (5) in varying distribution.Keywords
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