A Pulsed NMR System for Nuclear Thermometry Below 2 K
- 1 August 1973
- journal article
- research article
- Published by AIP Publishing in Review of Scientific Instruments
- Vol. 44 (8) , 1075-1082
- https://doi.org/10.1063/1.1686305
Abstract
A pulsed NMR system for platinum nuclear spin thermometry and for measurements of the nuclear spin‐lattice relaxation time τ1 has been developed. The nuclear free precession signal is detected with a fast linear detector and an RC integrator. The τ1 measurements were performed by the transient recovery method with the aid of automated circuitry multiplexing of the linear detector output into four separate integrators. The thermometer was tested between 10 mK and 2 K using a powdered platinum sample. Within the experimental accuracy of about 2% the amplitude of the nuclear free precession signal was found to be proportional to 1/T. The thermometer could be calibrated with the aid of the Korringa relation τ1T=κ, with κ=29.6 msec K. Thermal equilibrium problems of the τ1 measurements are discussed in detail.Keywords
This publication has 11 references indexed in Scilit:
- Construction and use of a pulsed copper nuclear magnetic resonance thermometerCryogenics, 1972
- The design and use of nuclear orientation thermometers employing54Mn and60Co nuclei in ferromagnetic hostsJournal of Low Temperature Physics, 1972
- Very-low-temperature static magnetic properties of certain metals possibly useful as magnetic thermometersJournal of Low Temperature Physics, 1971
- A dilution refrigerator with large cooling powerCryogenics, 1971
- Nuclear spin thermometry below 1 °KProceedings of the Royal Society of London. Series A. Mathematical and Physical Sciences, 1965
- An analysis of stagger-tuned pulse receiver systems with special reference to n.m.r. relaxation-time measurementsRadio and Electronic Engineer, 1964
- Nuclear magnetic resonance in platinumJournal of Physics and Chemistry of Solids, 1963
- Nuclear Magnetic Relaxation and Shift in PlatinumPhysical Review Letters, 1962
- Nuclear Magnetic Resonance in PlatinumPhysical Review Letters, 1962
- LIII. The rectification and observation of signals in the presence of noiseJournal of Computers in Education, 1951