5-Methyl-1,3,2-benzodithiaborole and related compounds
- 1 January 1974
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in Journal of the Chemical Society, Perkin Transactions 1
- p. 916-917
- https://doi.org/10.1039/p19740000916
Abstract
Reactions of 2-chloro-5-methyl-1,3,2-benzodithiaborole (I), obtained from toluene-3,4-dithiol and trichloroborane, with bis(trimethylsilyl)amine and tris(trimethylsilyl)amine have been studied. Tris-(5-methyl-1,3,2-benzodithiaborol-2-yl)amine, bis-(5-methyl-1,3,2-benzodithiaborol-2-yl)amine, and bis-(5-methyl-1,3,2-benzodithiaborol-2-yl)(trimethylsilyl)amine have been prepared. Tributyltin hydride converts (I) into 5-methyl-1,3,2-benzodithiaborole, which forms a stable complex with diethylamine.Keywords
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