A FACILE METHOD FOR THE PREPARATION OF 5-ALKOXY-1,4-DIKETONES
- 5 December 1978
- journal article
- research article
- Published by Oxford University Press (OUP) in Chemistry Letters
- Vol. 7 (12) , 1431-1434
- https://doi.org/10.1246/cl.1978.1431
Abstract
The title compoun\={a}s were prepared efficiently by Lewis acid catalyzed reaction of 1,2-bis(trimethylsiloxy)-1-cyclobutene with acetals, followed by addition of the Grignard reagent and ring cleavage of the resulting vis-diols with Pb(OAc)4.Keywords
This publication has 3 references indexed in Scilit:
- A novel ring-opening reaction. An improved method for reductive succinoylationThe Journal of Organic Chemistry, 1977
- Geminal acylation via pinacol rearrangement. Synthesis of spiro[4.n] ring systemsJournal of the American Chemical Society, 1977
- SCISSION OF STERICAIXY HINDERED vic-DIOLSCanadian Journal of Chemistry, 1960