Notizen: Synthesis of Isopropoxy-Chloro-Disulfane (ROSSCl) and its Reaction with Titanocene Pentasulfide to Give (RO)2S9
Open Access
- 1 April 1990
- journal article
- Published by Walter de Gruyter GmbH in Zeitschrift für Naturforschung B
- Vol. 45 (4) , 557-558
- https://doi.org/10.1515/znb-1990-0423
Abstract
Bis-alkoxy-disulfanes, ROSSOR, react with SCI, at 0 °C to give ROSSCl which yield the corresponding nonasulfanes, RO—S9—OR, on reaction with titanocene pentasulfide, (C5H5)2TiS5. Raman, mass, and NMR spectra of ROSSCl and (RO)2S9 (R = isopropyl) are reported.Keywords
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