Assignment of the NMR Parameters of the Branch-Point Trisaccharide of Ahylopectin Using 2-D NMR Spectroscopy at 500 MHz
- 1 January 1984
- journal article
- research article
- Published by Taylor & Francis in Journal of Carbohydrate Chemistry
- Vol. 3 (4) , 581-592
- https://doi.org/10.1080/07328308408057919
Abstract
The proton and carbon nuclear magnetic resonance spectroscopic data for methyl 4-O-α-d-glucopyranosyl-[6-O-a-u-glucopyranosyl]-β-d-glucopyranoside (1), a model for the branch-point trisacch-aride of amylopectin, have been analysed using 2-D-heteronuclear correlated spectroscopy. Similar data are presented for the related disaccharide structures methyl β-d-maltopyranoside and β-d-isomal topyranoside.This publication has 12 references indexed in Scilit:
- Nuclear Magnetic Resonance Spectroscopy in the Study of Mono- and OligosaccharidesPublished by Elsevier ,2008
- Synthesis of (6R)- and (6S)-D-glucose-6-2H through stereospecific photo-bromination of 1,6-anhydro-.BETA.-D-glucopyranose derivative.Agricultural and Biological Chemistry, 1983
- Carbon-13 Nuclear Magnetic Resonance Spectroscopy of MonosaccharidesPublished by Elsevier ,1983
- Experimental chemical shift correlation maps from heteronuclear two-dimensional nuclear magnetic resonance spectroscopy. II: Carbon-13 and proton chemical shifts of a-D-glucopyranose oligomersCanadian Journal of Chemistry, 1982
- Carbon-13 Nuclear Magnetic Resonance Spectroscopy of PolysaccharidesPublished by Elsevier ,1981
- Strukturaufklärung diastereomerer 1,3,6-Trioxacyclo-octansysteme durch gleichzeitige Relaxations- und DoppelresonanzexperimenteAngewandte Chemie, 1978
- Experimental chemical shift correlation maps in nuclear magnetic resonance spectroscopyJournal of the Chemical Society, Chemical Communications, 1978
- Halide ion catalyzed glycosidation reactions. Syntheses of .alpha.-linked disaccharidesJournal of the American Chemical Society, 1975
- 1H‐NMR Study of the Di‐Glucopyranoses in D2OBulletin des Sociétés Chimiques Belges, 1975
- Solutions to The Hidden-Resonance Problem in Proton Nuclear Magnetic Resonance SpectroscopyPublished by Elsevier ,1974