Preparation of some organotin compounds containing methylthio, phenylthio, and pentafluoro-phenylthio groups
- 15 January 1968
- journal article
- Published by Canadian Science Publishing in Canadian Journal of Chemistry
- Vol. 46 (2) , 211-215
- https://doi.org/10.1139/v68-033
Abstract
The new compounds n-Bu3SnSR, n-Bu2Sn(SR)2, where R = Me, Ph, or C6F5, and Ph3SnSC6F5 have been prepared and characterized. The fracture of the Sn—S bond with iodine has been examined and affords a quantitative method for analysis of compounds containing a Sn—S bond. The 1H and 19F n.m.r. have been studied; frequencies characteristic of the C6F5S— group in the infrared spectra have been tabulated.Keywords
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