A Convenient Method for the Synthesis of 1-Adamantyldichlorophosphine

Abstract
1-Adamantyldichlorophosphine is obtained in good yield by reduction of 1-adamantyldichlorophosphine sulfide with triphenylphosphine in toluene. It can be quantitatively reduced to 1-adamantylphosphine with lithium alanate in ether.

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