Enantioselective Construction of Vicinal Stereogenic Quaternary Centers by Dialkylation: Practical Total Syntheses of (+)- andmeso-Chimonanthine

Abstract
All three stereoisomers of the hexacyclic 3a,3a′-bispyrrolidino[2,3-b]indoline moiety found in complex indole alkaloids can be prepared, as illustrated by total syntheses of meso-chimonanthine (1) and (+)-chimonanthine (2). A rare example of high diastereoselectivity arising from the combination of a prostereogenic enolate with a chiral electrophile containing a sp3 carbon atom is the key feature of the asymmetric synthesis of the C2 stereoisomer.

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