Organoimido complexes of tungsten(IV) containing π-alkene and π-acetylene ligands. The X-ray crystal structure of dichloro(diphenylacetylene)phenylimidobis(trimethylphosphine)tungsten(IV), [WCl2(NPh)(PhCCPh)(PMe3)2]

Abstract
Reduction of [WCl3(NPh)(PMe3)2)] under ethylene or propene leads to the complexes [WCl2(NPh)(π-alkene)(PMe3)2], and reaction of [WCl2(NPh)(PMe3)3] with a variety of acetylenes gives [WCl2(NPh)(π-acetylene)(PMe3)2]; the structure of [WCl2(NPh)(PhCCPh)(PMe3)2] has been established by X-ray crystallography.

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