Elemental fluorine. Part 6. Fluorination of cyclic 1,3-diketones and related compounds
- 1 January 1996
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in Journal of the Chemical Society, Perkin Transactions 1
- No. 18,p. 2271-2275
- https://doi.org/10.1039/p19960002271
Abstract
Direct fluorination of cyclic 1,3-diones gives 2-mono- and 2,2-di-fluorinated products. The monofluorinated compounds crystallise in their enol forms and the difluorinated compounds form stable monohydrates whose crystal structures have been elucidated. Direct fluorination of phlorogulcinol in formic acid yields 1,1,3,3,5,5-hexafluoro-2,2,4,4,6,6-hexahydroxycyclohexane.Keywords
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