Heteronuclear dipolar modulated chemical shift spectra for geometrical information in polycrystalline solids
- 15 November 1976
- journal article
- research article
- Published by AIP Publishing in The Journal of Chemical Physics
- Vol. 65 (10) , 4093-4098
- https://doi.org/10.1063/1.432863
Abstract
A double resonance multiple pulse nuclear magnetic resonance experiment is proposed and demonstrated which allows the use of heteronuclear dipolar interactions to determine geometrical, orientational, and motional information in polycrystallinesolids.13C–1H double resonance experiments are performed in polycrystalline benzene and calcium formate to demonstrate the capabilities of the technique in its present form.Keywords
This publication has 16 references indexed in Scilit:
- Heteronuclear spin dynamics using multiple pulse NMR techniquesThe Journal of Chemical Physics, 1976
- Characterization of the methylene 13C chemical shift tensor in the normal alkane n-C20H42The Journal of Chemical Physics, 1976
- Structure determination by dipolar coupling measurements of dilute nuclear spins in a polycrystalline solidThe Journal of Chemical Physics, 1975
- Resolved Dipolar Coupling Spectra of Dilute Nuclear Spins in SolidsPhysical Review Letters, 1975
- Carbon-13 chemical shielding tensors in calcium formateJournal of the American Chemical Society, 1974
- Analysis of multiple pulse NMR in solids. IIThe Journal of Chemical Physics, 1974
- A Simple, Low Power, Multiple Pulse NMR SpectrometerReview of Scientific Instruments, 1972
- Coherent Averaging Effects in Magnetic ResonancePhysical Review B, 1968
- Approach to High-Resolution nmr in SolidsPhysical Review Letters, 1968
- Multiple-Pulse NMR ExperimentsThe Journal of Chemical Physics, 1968