A New and Easy Synthesis of Silylated Furanoid Glycals in One Step from Nucleosides
- 1 January 1994
- journal article
- research article
- Published by Georg Thieme Verlag KG in Synthesis
- Vol. 1994 (10) , 1037-1038
- https://doi.org/10.1055/s-1994-25633
Abstract
Silylated furanoid glycals are synthesized in high yields by elimination of the nucleobase in thymidine (1a) and 5′-O- (tert-butyldiphenylsilyl)thymidine (1b) on treatment with 1,1,1,3,3,3-hexamethyldisilazane (HMDS) in the presence of ammonium sulfate at reflux temperature for 2 hours.Keywords
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