High irreversibility fields and current densities in single crystals and melt-textured samples
- 1 September 1997
- journal article
- research article
- Published by American Physical Society (APS) in Physical Review B
- Vol. 56 (10) , 6308-6319
- https://doi.org/10.1103/physrevb.56.6308
Abstract
single crystals and melt-textured samples were prepared in reduced atmospheres starting from the Nd-poor side of the phase diagram in order to minimize the Nd/Ba substitution and the second phase content. Current density and irreversibility field were measured as a function of temperature and angle between the axis and applied field direction in samples with different impurity and oxygen contents. Current density vs field shows a pronounced peak effect which results from small clusters of oxygen vacancies, whereas a second peak is related to the twin structure. The current density at 77 K is for fields up to 4 T above and reaches values of in the peak at 2.1 T. The irreversibility fields parallel to the axis reach 13.4 and 11.8 T at 77 K in pure and homogeneous single crystals and melt-textured samples, respectively. These extremely high values, which are caused by the twin structure, decrease to 10 and 8 T, respectively, if the current is optimized. The correlation and interference between and in the presence of weakly and strongly interacting defects such as small clusters of oxygen vacancies and Nd-422 precipitates, respectively, as well as the influence of the twin structure are analyzed and discussed.
Keywords
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