Highly substituted dienes from butyne-1,4-diol. A one-flask synthesis and the mechanism of formation of 3-(N,N-diethylamino)-2-phenylsulphinylbutadiene
- 1 January 1982
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in Journal of the Chemical Society, Chemical Communications
- No. 12,p. 665-666
- https://doi.org/10.1039/c39820000665
Abstract
When 4-acetoxybut-2-yn-1-ol is treated with benzenesulphenyl chloride and triethylamine, followed by diethylamine, 3-(N,N-diethylamino)-2-phenylsulphinylbutadiene is produced, in a multistep process, in 90% overall yield.Keywords
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