Structure and ordering in metal cyanide lattices: the use of doubly labelled cyanide (13C–15N) to simplify the13C MAS NMR spectrum
- 1 January 1992
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in Journal of the Chemical Society, Chemical Communications
- No. 24,p. 1800-1802
- https://doi.org/10.1039/c39920001800
Abstract
The relatively simple procedure of incorporating doubly labelled 13C–15N into metal cyanide lattices gives a significant simplification of the MAS NMR spectrum, yielding readily interpretable structural information, and the first example of 13C–63,65Cu J coupling constants in the solid state, for NMe4Cu(I)Zn(CN)4.Keywords
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