Enzyme‐linked immunosorbent (ELISA) determination of aflatoxin B1in peanut butter: Collaborative trial

Abstract
Fourteen laboratories in the United Kingdom participated in a collaborative trial of a commercially available ELISA test kit for the determination of aflatoxin B1 in peanut butter. Each laboratory carried out six replicate analyses of each of six individual samples. Collaborators received a control, uncontaminated sample, together with samples prepared by blending naturally‐contaminated and control material to give target levels of 8 μg/kg, 25 μg/kg and 75 μg/kg. Two of these samples (8 μg/kg and 25 μg/kg) were supplied as undisclosed duplicates. The repeatabilities of the assay ranged from 6.2 to 16.7 μg/kg. The reproducibilities for aflatoxin B1 concentrations in naturally‐contaminated samples ranged from 3.6 to 18.7 μg/kg using uncontaminated peanut butter as a reference blank. Modifications to the format of the commercial kit were recommended as a result of the collaborative trial.

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