A novel hexakis(tetrathiafulvalene) derivative: synthesis, structure and electrochemical properties
- 21 February 2000
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in Chemical Communications
- No. 5,p. 331-332
- https://doi.org/10.1039/a909882h
Abstract
The hexakis(TTF) derivative 3 has been synthesised in 89% yield by six-fold reaction of the thiolate anion of reagent 2 with hexakis(bromomethyl)benzene: the solution electrochemistry of 3 shows sequential formation of the hexa- (radical cation) and the dodecacation species, and spectroelectrochemistry shows interacting radical cations; the X-ray crystal structure of 3 is reported.Keywords
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