Molybdenum polysulfide hollow microtubules grown at room temperature from solution

Abstract
Reaction of (NH4)2MoS4 and (NH2OH)2·H2SO4 under hydrothermal conditions led to the new compound (NH3 - OH)3.9MoS4.8 I, which crystallises from acetone solution producing hollow tubules of nanoscopic size (50–500 nm diameter, 0.1–20 μm length); thermal decomposition of I led to the formation of highly dispersed tubular MoS2.

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