Messung der Krypton-85-Aktivität der atmosphärischen Luft / A Method for Measurement of the Krypton-85-content in the Atmosphere
Open Access
- 1 August 1975
- journal article
- Published by Walter de Gruyter GmbH in Zeitschrift für Naturforschung A
- Vol. 30 (8) , 959-961
- https://doi.org/10.1515/zna-1975-0806
Abstract
To measure the Kr-85 content in the atmosphere we developed a simple method. Within a time internal of five to ten days (depending on the moisture of the air) five to ten m 3 of air (NTP) are pumped through activated carbon (pressure 300 torr, temperature 77 °K). When sampling time is over, the carbon is heated to 470 °K. This gives a gas sample of 4 1 with more than 90% of the atmospherical krypton in 3 hours. With a further step of enrichment, the volume of the sample is reduced to 100 ml. The final separation of krypton from O2 , N2 , CO, CO2 and Xe is made by gaschromatography at room temperature with methane as eluent gas (duration 25 min). The Kr-fraction is transported to a proportional counter (200 ml). The overall yield is 90%. The overall error of the Kr-85 content is near 1%. Data are given for the time of 15. 6. 1973 to 29. 12. 1974.Keywords
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