Synthesis of PbS nanocrystallites using a novel single molecule precursors approach: X-ray single-crystal structure of Pb(S2CNEtPri)2
- 1 January 1997
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in Journal of Materials Chemistry
- Vol. 7 (6) , 1011-1016
- https://doi.org/10.1039/a608579b
Abstract
The synthesis and characterisation of some lead(ii) dithiocarbamato complexes Pb(S 2 CNRR′) 2 is reported. These compounds were used as single molecule precursors to produce nanocrystalline PbS by their thermolysis in trioctylphosphine oxide. The optical and morphological properties of the resulting PbS nanocrystallites were investigated; the influence of experimental parameters, such as precursor, growth time and temperature, on the final nanodispersed materials is also reported.Keywords
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