A Convenient One-Flask Preparation of Di-t-butyl Iminodicarbonate: A Versatile Gabriel Reagent
- 1 January 1987
- journal article
- research article
- Published by Georg Thieme Verlag KG in Synthesis
- Vol. 1987 (03) , 275-276
- https://doi.org/10.1055/s-1987-27914
Abstract
An improved synthesis of di-t-butyl iminodicarbonate from formamide and di-t-butyl dicarbonate with dimethylaminopyridine as a catalyst followed by aminolytic removal of the formyl group is described as well as a few applications related to the synthesis of primary amines.Keywords
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