Single-crystal electronic and electron spin resonance spectra of bis-(diethylenetriamine)copper(II) nitrate

Abstract
The polarised single-crystal electronic spectra and e.s.r. spectrum of Cu(dien)2(NO3)2 are interpreted in C2 effective symmetry, with a dz2 ground-state. This yields the one-electron orbital sequence dz2 > dx2y2, dxy > dxz, dyz; the precise order of the dx2y2 and dxy levels is not certain, but that with the dx2y2 above the dxy level is preferred. The low energy of the dx2y2dz2 transition reflects the small ‘ tetragonal ’ distortion arising from the out-of-plane chelation of diethylenetriamine. A method is given for calculating the molecular g-values, for rhombic symmetry, from data on crystals containing four inequivalent orientations.

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