Convenient synthesis of α-acylamino aldehydes
- 1 January 1979
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in Journal of the Chemical Society, Chemical Communications
- No. 2,p. 79-80
- https://doi.org/10.1039/c39790000079
Abstract
The reduction by di-isobutylaluminium hydride of N-blocked amino acid imidazolides gives good yields of α-acylamino aldehydes, the optical purity of which is higher than those previously reported, but a check of one aldehyde prepared showed only 60% optical purity; the chemical shifts at the aldehydo 13C and 1H resonances are reported.Keywords
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