Oxidation of Primary Aliphatic Amines toC-Nitroso Dimers
- 1 January 1988
- journal article
- research article
- Published by Georg Thieme Verlag KG in Synthesis
- Vol. 1988 (10) , 808-810
- https://doi.org/10.1055/s-1988-27717
Abstract
A biphasic system of ethyl acetate or dichloromethane and water containing sodium percarbonate (Na2CO3·3/2 H2O2), sodium hydrogen carbonate and N,N,N′,N′-tetraacetylethylenediamine oxidizes primary aliphatic amines to aliphatic C-nitroso dimers in most cases in good to excellent yields.Keywords
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