Synthesis of Unsaturated Tricyclic Lactones. The Coupling of the Enol Triflate of β-Keto Lactones with Lithium Dimethylcuprate

Abstract
The anions of selected β-keto lactones were transformed into their corresponding enol triflates. These enol triflates were coupled with lithium dimethylcuprate to afford tricyclic unsaturated /aciones, key intermediates for the synthesis of the biologically important natural product forskolin.

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