Quantitative Analysis by X-Ray Diffraction of the Inclusion Complex Formed byd-Limonene in aβ-Cyclodextrin/Maltodextrin Mixed Powder

Abstract
The level of the inclusion complex between β-Cyclodextrin (β-CD) and d-Limonene in a pure β-CD and β-CD/maltodextrin mixed powder was measured by X-ray diffraction. The relative integral intensity at 2θ=5-7° and 11-12° correlated well with the molar fraction of d-Limonene to the total moles of β-CD and the maltodextrin mixture. Solid state (13)C-CP/MAS NMR results correlated well with those by X-ray diffraction.

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