13C nuclear magnetic resonance spectra of NN-dimethylformamide in aqueous acid solution. Evidence for predominant O-protonation at all acidities

Abstract
The observation of a doublet methyl signal in the 13C n.m.r. spectrum of NN-dimethylformamide from 0–100% H2SO4 demonstrates that the predominant protonated form at all acidities is the O-protonated amide.

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