Lifting the lid on metatungstate. 1H and 183W NMR study of the six electron reduced anion [(H)2{WIV3(OH2)3}WVI9O34(OH)3]3−
- 1 January 1999
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in Chemical Communications
- No. 6,p. 533-534
- https://doi.org/10.1039/a900088g
Abstract
The distribution of the eleven protons present in a six-electron reduced form of metatungstate, [(H)2{WIV 3- (OH2)3}WVI 9O34(OH)3]3–, in dry CD3CN is mapped by 1H and 183W NMR, allowing assessment of structural changes which accompany reduction.Keywords
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