Use of shift reagent with diastereomeric MTPA esters for determination of configuration and enantiomeric purity of secondary carbinols in 1H NMR spectroscopy
- 1 January 1976
- journal article
- Published by Elsevier in Tetrahedron
- Vol. 32 (12) , 1363-1367
- https://doi.org/10.1016/0040-4020(76)85011-9
Abstract
No abstract availableKeywords
This publication has 14 references indexed in Scilit:
- Determination of enantiomeric purity using chiral lanthanide shift reagentsJournal of the American Chemical Society, 1974
- Chiral 1-deuterio alcohols. Synthesis and determination of enantiomeric purity by chiral lanthanide nmr shift reagents.Tetrahedron Letters, 1973
- Paramagnetic lanthanide shift reagents in NMR spectroscopy: Principles, methodology and applicationsProgress in Nuclear Magnetic Resonance Spectroscopy, 1973
- Lanthanide shift reagents for nuclear magnetic resonance spectroscopyChemical Reviews, 1973
- Correlation of configuration and fluorine-19 chemical shifts of .alpha.-methoxy-.alpha.-trifluoromethylphenyl acetate derivativesThe Journal of Organic Chemistry, 1973
- Asymmetric reductions with chiral reagents from lithium aluminum hydride and (+)-(2S,3R)-4-dimethylamino-3-methyl-1,2-diphenyl-2-butanolThe Journal of Organic Chemistry, 1973
- Nuclear magnetic resonance enantiomer regents. Configurational correlations via nuclear magnetic resonance chemical shifts of diastereomeric mandelate, O-methylmandelate, and .alpha.-methoxy-.alpha.-trifluoromethylphenylacetate (MTPA) estersJournal of the American Chemical Society, 1973
- Reversal in stereoselectivity depending upon the age of a chiral lithium alkoxyaluminohydride reducing agentJournal of the American Chemical Society, 1972
- .alpha.-Methoxy-.alpha.-trifluoromethylphenylacetic acid, a versatile reagent for the determination of enantiomeric composition of alcohols and aminesThe Journal of Organic Chemistry, 1969
- Modern Methods for the Determination of Optical PurityPublished by Wiley ,1967