Abstract
The syntheses of deutero‐labelled di‐(2‐ethylhexyl)adipate (DEHA), mono‐(2‐ethylhexyl) adipate (MEHA), 2‐ethylhexan‐1‐ol, 2‐ethylhexanoic acid, 2‐ethyl‐5‐ketohexanoic acid, 3‐ethyl‐6‐methyltetrahydro‐2H‐pyran‐2‐one and 2‐ethylhexanedioic acid are described. All compounds were perdeutero‐labelled in the ethyl group. The title compound, DEHA, was used in a human dosing study.

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