The Carbon-13 Magnetic Resonance Spectrum of an Organic Peroxide

Abstract
Phenanthrene ozonide and methanol combine under acid catalysis to produce a 1:1 adduct, mp 180–181°, assigned structure 1 on the basis of C-H analysis and infrared spectrum.1,2 Although β,β′-dihydroxyalkylperoxides have been isolated from equilibrium mixtures of aldehydes and hydrogen peroxide, they are rarely if ever as thermally stable as the phenanthrene ozonide:methanol adduct.3

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