Natural acetylenes. Part XXXII. A synthesis of crepenynic acid (octadec-9-en-12-ynoic acid)
- 1 January 1971
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in Journal of the Chemical Society C: Organic
- p. 1156-1158
- https://doi.org/10.1039/j39710001156
Abstract
Methyl crepenynate has been synthesised from non-3-yn-1-yl-triphenylphosphonium bromide (obtained from hept-1-yne via non-3-yn-1-ol and 1-bromonon-3-yne) and the C9 aldehyde-ester with butyl-lithiumin ether, and from it crepenynic acid was obtained by alkaline hydrolysis.Keywords
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