Abstract
The reaction between gaseous ammonia and sulfur chlorides (S/sub 2/Cl/ sub 2/ and SCl/sub 2/) was studied under various conditions of temperature, flowrate of ammonia, concentration and type of sulfur chloride, solvent, and duration of run, for the purpose of determining the optimum conditions for the preparation of S/sub 4/N/sub 4/ and S/sub 7/NH. Adsorption-column chromatography on alumina and silica gel columns was employed for the quantitative separation of the reaction products. (auth)

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