Barton Decarboxylation of Cubane-1,4-dicarboxylic Acid: Optimized Procedures for Cubanecarboxylic Acid and Cubane

Abstract
Cubane-1,4-dicarboxylic acid (3) and its monomethyl ester 2 were converted to cubanecarboxylic acid (4) and cubane (5), respectively, by homolytic decomposition of the corresponding thiohydroxamic esters.

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